The Discover SP Microwave synthesizer (CEM) allows for rapid heating of solvents up to 300 °C and pressures up to 300 psi. Reaction vessels can be prepared in a glovebox and will maintain inert environment while capped allowing for air free synthesis. Reaction conditions are monitored over time through software and can be saved for comparison between syntheses. Reactions are rapidly cooled down following synthesis by flowing compressed air around the reaction vessel. The system is also equipped with an autosampler accessory that enables automatic handling of reaction vessels allowing for different experiments to be programmed and performed automatically.